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51.
Abstract: The densities of CO2 inclusions in minerals are commonly used to determine the crystallizing conditions of the host minerals. However, conventional microthermometry is difficult to apply for inclusions of small size (< 5–10 μm) or low density. Raman analysis is an alternative method for determining CO2 density, provided that the CO2 density–Raman shift relation is known. This study aims to establish this CO2 density–Raman shift relation by using CO2 inclusions synthesized in fused silica capillaries. By using this newly-developed synthetic technique, we formed pure CO2 inclusions, and their densities were determined by microthermometry. The Raman analysis showed that the relation between CO2 density (D in g/cm3) and the separations (Δ in cm?1) between the two main bands (i.e. Fermi diad bands) in CO2 Raman spectra can be represented by a cubic equation: D (g/cm3)=0.74203(?0.019Δ3+5.90332Δ2?610.79472Δ+21050.30165)?3.54278 (r2=0.99920). Our calculated D value for a given Δ is between those obtained from two previously-reported equations, which were derived from different experimental methods. An example was given in this study to demonstrate that the densities of natural CO2 inclusions that could not be derived from microthermometry could be determined by using our method. 相似文献
52.
海洋沉积物中残留的硅壳、甲藻孢囊、类脂类化合物及生物硅等生态参数被广泛应用于反演和指示海洋古环境特征.本研究通过测定烟台四十里湾表层沉积物中的硅藻化石、甲藻孢囊、菜籽甾醇、甲藻甾醇及生物硅5种生态参数,比较不同生态参数的相关性及它们在反演海洋环境中的功能差异,建立了多参数综合应用的研究方法.研究发现,沉积物中的硅壳丰度与菜籽甾醇含量及生物硅含量存在明显正相关关系(P＜0.05),菜籽甾醇含量与生物硅含量可以较好的佐证与提高沉积物中硅壳对硅藻生物量指示的准确性;甲藻孢囊与甲藻甾醇含量相关性不明显(P＞0.05),相较而言,甲藻甾醇可以更准确的反演甲藻的生物量.因此,生物与化学参数的结合应用不仅可以提高生物量指示的精确性,而且有助于从物种组成角度更好的了解藻类对环境变化的响应特征. 相似文献
53.
54.
A modified method for biogenic silica determination 总被引：1，自引：0，他引：1
We describe a modified method for the determination of biogenic silica (BSi) in lacustrine sediment samples with BSi concentrations
>0.5% SiO2 (detection limit). To speed up the leaching procedure (48 samples per day), we suggest the use of Teflon autoclaves that
can be left unattended (no stirring of the solution) for 3 h at 100°C in an oven. We suggest a volume correction by Na measurement
to account for volume errors during pipetting off a hot solution. We also propose to carry out a correction for minerogenic
silica by the simultaneous determination of Al in the leachate. Analytical precision and accuracy of the proposed method are
2.4% (relative standard deviation) and 70–110% recovery (relative to the mean of four international reference sediment samples),
respectively. Additionally, we demonstrate that pre-treatment of the samples with H2O2 and/or HCl prior to alkaline leaching is not necessary for all samples. Due to the great diversity of lacustrine and marine
sediments, however, the pre-treatment procedure should be tailored for samples from different sites. 相似文献
55.
We present a paleolimnological record spanning the Holocene from a small lake on Russell Island (Lake PW02), in the central
Canadian Arctic Archipelago (74.07° N, 97.77° W, 182 m asl). Fragilarioid diatom types in the genera Pseudostaurosira, Staurosira and Staurosirella constitute >90% of valves in fossil samples. Using modern biogeographic data which specify the temperature optima of the
Fragilarioid diatom taxa, we present new inferences about the timing of paleoclimatic changes in the central Arctic islands.
The early Holocene was characterized by maximum values for sediment organic matter, and lower ratios of Staurosirella pinnata to Staurosira construens v. venter, suggesting warm summer air temperatures between about 9500−6500 cal year BP. Influxes of biogenic silica and diatom valves
decreased following 4000 cal year BP, the sediment accumulation rate slowed and diatom taxa of the littoral zone diversified,
suggesting cooler summers and more persistent lake ice. Variations in the species composition of the assemblages indicate
paleoclimatic changes that are in broad agreement with other paleoenvironmental records from the Arctic including melt records
from the Agassiz Ice Cap. Although autecological data remain incomplete for Fragilarioid taxa, our results indicate differences
in these taxa in responses to paleoenvironmental change and underline the potential for the increased use of these taxa in
paleoenvironmental reconstructions. The record from Lake PW02, as in other records from Arctic lakes with low algal diversity
throughout the Holocene, shows a pronounced increase in diatom diversity since the 1920s, and diatom production since the
1970s far exceeds any recorded during the Holocene. 相似文献
56.
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59.
Lisa E. Collins William BerelsonDouglas E. Hammond Angela Knapp Richard SchwartzDoug Capone 《Deep Sea Research Part I: Oceanographic Research Papers》2011,58(8):898-914
Moored sediment traps were deployed from January 2004 through December 2007 at depths of 550 and 800 m in San Pedro Basin (SPB), CA (33°33.0′N, 118°26.5′W). Additionally, floating sediment traps were deployed at 100 and 200 m for periods of 12-24 h during spring 2005, fall 2007, and spring 2008. Average annual fluxes of mass, particulate organic carbon (POC), ??13Corg, particulate organic nitrogen (PON), ??15N-PON, biogenic silica (bSiO2), calcium carbonate (CaCO3), and detrital material (non-biogenic) were coupled with climate records and used to examine sedimentation patterns, vertical flux variability, and organic matter sources to this coastal region. Annual average flux values were determined by binning data by month and averaging the monthly averages. The average annual fluxes to 550 m were 516±42 mg/m2 d for mass (sdom of the monthly averages, n=117), 3.18±0.26 mmol C/m2 d for POC (n=111), 0.70±0.05 mmol/m2 d for CaCO3 (n=110), 1.31±0.21 mmol/m2 d for bSiO2 (n=115), and 0.35±0.03 mmol/m2 d for PON (n=111). Fluxes to 800 and to 550 m were similar, within 10%. Annual average values of ??13Corg at 550 m were −21.8±0.2‰ (n=108), and ??15N averages were 8.9±0.2‰ (n=95). The timing of both high and low flux particle collection was synchronous between the two traps. Given the frequency of trap cup rotation (4-11 days), this argues for particle settling rates ≥83 m/d for both high and low flux periods. The moored traps were deployed over one of the wettest (2004-2005, 74.6 cm rainfall) and driest (2006-2007, 6.6 cm) rain years on record. There was poor correlation (Pearson's correlation coefficient, 95% confidence interval) of detrital mass flux with: Corg/N ratio (r=0.10, p=0.16); ??15N (r=−0.19, p=0.02); and rainfall (r=0.5, p=0.43), suggesting that runoff does not immediately cause increases in particle fluxes 15 km offshore. ??13Corg values suggest that most POC falling to the basin floor is marine derived. Coherence between satellite-derived chlorophyll a records from the trap location (±9 km2 resolution) and SST data indicates that productivity and export occurs within a few days of upwelling and both of these parameters are reasonable predictors of POC export, with a time lag of a few days to 2 weeks (with no time lag—SeaWiFS chlorophyll a and POC flux, r=0.25, p=0.0014; chlorophyll a and bSiO2 flux, r=0.28, p=0.0002). 相似文献
60.
四川盆地碳酸盐岩储层为我国主要海相储层之一。通过分析四川盆地碳酸盐岩中硅质的宏观、微观特征,提出硅质以互层、混积、充填、交代的形式存在于碳酸盐岩中。互层硅质、充填硅质和交代硅质中二氧化硅来源以火山喷发为主,但后期沉积机制不同;混积硅质中二氧化硅来源于陆源碎屑,对物源方向具有一定的指向意义,沉积机制为陆源混积。互层硅质、充填硅质、交代硅质对储层形成具有双重意义,混积硅质对储层形成起严重破坏性作用。 相似文献